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The coupling reaction of aryl iodides with acetylacetone or ethyl cyanoacetate beneath catalysis of CuI/l-proline works at ­relatively mild circumstances to provide 3-aryl-2, 4-pentanediones and α-aryl cyanoacetates in reasonable to good yields. Substituted carbazol-4-ones and 3,4-dihydrocyclo-pental indole-1-ones may very well be prepared in good yields by way of the intra­molecular coupling response of N-2-iodoaryl enaminones in the presence of CuI/l-proline beneath mild response situations. ...

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With PM below circulate injection analysis conditions, the LOD was 10 μm Pro-NO. To quantify L-proline, high-pressure liquid chromatography was performed using an Agilent 1200 sequence equipped with an Eclipse Plus C18, 3.5 μm, 4.6 × one hundred mm, and a diode array detector (DAD G1321A) through O-phthalaldehyde and 9-fluorenylmethyl chloroformate derivative response in line with the high-velocity amino acids manufacturer near me-acid analysis on 1.Eight μm reversed-phase columns instruction o...

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